A cooperative-learning jigsaw-style activity was developed to create opportunities for introductory organic chemistry students to discuss and decipher [superscript 1]H NMR spectra. Students cooperatively interpreted spectra that contained both pure and mixed solvents, building consensus through explanation and argumentation on what each spectrum…

The demand for sustainable synthetic methods in modern industry has been increasing rapidly due to the requirements of environmental protection and energy conservation, which has brought organic electrochemical synthesis to the forefront nowadays. Here, a two-part laboratory experiment has been designed to train undergraduates in comprehending and…

This laboratory practice is intended for undergraduate students of chemistry, physics, biology, and engineering, to illustrate the simple concepts behind dye-sensitized solar cells (DSSCs), and how basic chemistry can be translated into a practical application through the use of microcontrollers. Unlike commercial counterparts, one of the main…

Students learned the principles and practice of photometry through project-based learning. They addressed the challenge of measuring the unknown concentration of a colored substance using a photometer they were required to design, build, and test. Then, they used that instrument to carry out the experiment and fulfill the challenge. A photometer…

This paper describes a student laboratory in the Unit Operations Laboratory at the Colorado School of Mines: air separation by pressure swing adsorption. The flexibility of the system enables students to study the production of enriched nitrogen or oxygen streams. Automatic data acquisition permits the study of cycle steps and performance.…

A novel method of measuring the coefficients of kinetic and rolling friction is proposed. The method is simple to implement and reliable. Samples of measurements and calculations are presented.

Gas-phase nitrogen oxides are important in the formation of tropospheric ozone. NO[subscript x] (NO and NO[subscript 2]) as well as tropospheric ozone have been shown to have negative effects on human health. Therefore, accurately measuring NO[subscript x] concentrations in the atmosphere is important. In this laboratory experience, students…

This study aims to design a mechanism with which the density of any solid or liquid can be determined without measuring its mass and volume in order to help students comprehend the concept of density more easily. The "solidensimeter" comprises of two scaled and nested glass containers (graduated cylinder or beaker) and sufficient water.…

This work describes a simple experiment to measure the resistor temperature as a function of the applied power and proves that it is an efficient way to introduce some important physical concepts in classroom, including the Joule's first law, hot-spot temperature, thermal resistance, thermal dissipation constant, time constant and the Newton's law…

The development and evaluation of a 6-hours laboratory class, based on capillary electrophoresis (CE) and the detection of microbial contaminants, is described. It can be easily scaled up or down, to suit class sizes up to 188 and completed in a shorter time scale. CE uses narrow-bore fused-silica capillaries to separate a complex array of large…

The separation of chamazulene from hydrophilic contaminants present in blue tansy oil provides a visually engaging example of two common techniques: extraction and thin-layer chromatography (TLC). This application uses liquid CO[subscript 2] as a lipophilic solvent to pull a brilliant blue hydrocarbon molecule, chamazulene, out of or through a…

A low-cost alternative to the typical scientific laboratory water bath or a hot plate stirrer water bath is proposed. Readily available immersion circulators have been developed for sous vide cooking. These precision cookers are designed to maintain water at an exact temperature and thus are well-suited for the similar laboratory requirements of a…

This laboratory experiment leverages the pedagogical value and multidisciplinary nature of biodiesel production from vegetable oil to introduce students to continuous-flow chemistry, a modern and rapidly growing approach to chemical synthesis. An interdisciplinary approach exposes students to the practical and conceptual aspects of modern…

Expensive, highly reflective barium sulfate plates are typically used to obtain solid-state UV-vis electronic spectra. Through normal laboratory use these plates become dirty, chip, and break, thus requiring replacement. An alternative to purchasing new plates is to make your own by combining a mechanical stabilizer, such as gum arabic, with…

A teaching laboratory experiment is described where students prepare in vitro transcription reactions of a fluorescent RNA aptamer, named Broccoli, and observe the production of the aptamer in real-time on a fluorescence plate reader. Alternate visualization methods with minimal costs are also described for laboratories lacking this…