Amides are usually prepared using amines and acyl halides, which often implies a two-step procedure. Alternatively, coupling reagents can be used in a single-step reaction with good yields, which seems to be suitable for organic chemistry laboratory classes. This work was designed to synthesize "N"-hexylcinnamamide through a one-step…

In light of the COVID-19 pandemic situation, the separation of the primary colors of ink markers and food coloring was performed using a simplified column chromatography setup at home to accomplish the educational outcome of the course. The virtual class instruction, for the students enrolled in the "Organic Techniques Laboratory"…

Light emitting diodes have been used to determine Planck's constant in introductory physics laboratories. One common method relies on the energy of the light emitted by the LED and its relation to the energy gap in the solid of which the diode is composed. However, there could be a problem with the data that are collected for this experiment. For…

In this article, we examine the rotation angle dependence of a hand-made fan-type variable capacitor for use in physics experiments in university classes. We made two circular bakelite plates, and the two terminal plates of the capacitor were 90° fan-type copper disks. The capacitance varied linearly with the rotation angle. The standard deviation…

The prompt transfer of cutting-edge science into students' curricula is a challenging task. Often research experiments are too complex or expensive to be translated into a secondary or tertiary education setting. Herein, we introduce a laboratory experiment that translates the recently developed research technique of a wavelength dependent,…

Acid--base chemistry is an important and challenging topic for virtually all chemistry students. Recent works have focused on conceptually linking molecular and symbolic representations to experimental evidence for many chemical concepts. In this work we describe a laboratory exercise designed to address students' conceptual challenges regarding…

This paper describes an upper-division undergraduate exercise involving the synthesis and iodometric and infrared spectroscopic analysis of the peroxide double salt [Zn(NH[subscript 3])[subscript 4]][Mo(O[subscript 2])[subscript 4]]. Here, iodometric methods are employed to determine the peroxide content of the compound, a procedure widely used…

This paper describes a first-year undergraduate exercise involving the synthesis of an "unknown" polyiodide salt, (NMe[subscript 4])[I[subscript 5]], and the determination of its formula using the classic iodine-thiosulfate (iodometric) titration. The exercise introduces students to simple synthetic and titrimetric techniques, assists…

The acoustic resonance in four glass Helmholtz resonators with diameters of 70, 52, 40, and 32 mm was detected in the frequency range of 360 to 1700 Hz using the simple experimental setup presented in this paper. The measured amplitudes of acoustic pressure required correction since the sound pressure amplitude of the loudspeaker used was not…

Introductory physics laboratory experiments have typically been employed to reinforce classroom instruction instead of teaching students experimental design. Recent research has shown that lab experiments that focus on experimental practices are more effective at teaching students physics concepts. The experiment described in this paper has been…

This paper describes a laboratory experiment that was designed to improve engineering education in fluids and hydrology courses. The laboratory module is part of a broader effort to enhance the undergraduate engineering laboratory curriculum to incorporate modern pedagogical methods and to improve a defined set of student outcomes. The…

The bromination of six isomeric alcohols is adapted to a discovery-based organic chemistry laboratory experiment, whereby students are provided an alcohol starting material and are charged with determining the product or product mixture produced using relevant spectroscopic data. The experiment solidifies NMR analysis skills while reinforcing the…

We have developed a new foundation-level course at our institution that links the concept of chemical equilibria from four of the traditional subdisciplines (analytical, biochemistry, inorganic, and physical). The course, entitled Solution and Solid State Chemistry (CHEM 210), is designed to serve our chemistry and biochemistry majors, as well as…

This laboratory experiment introduces upper-division undergraduate analytical chemistry students to liquid chromatography-tandem mass spectrometry (LC-MS/MS) in a forensic application: the analysis of cocaine and metabolites of cocaine in simulated serum ostensibly from drug overdose victims. For this investigation, students developed the…

We propose an apparatus that emulates the experiment used by Geiger and Marsden in 1913 to investigate alpha particles (Rutherford) scattering. Using a widely available fused deposition modelling 3D-printer, we built a compartmented and easily assembled educational instrument. The whole apparatus is composed of a 3D-printed chamber and an…