This article highlights the multianalytical study of exuded liquid from an ancient Egyptian sealed alabaster vase by Master's students in an applied chemistry for cultural heritage course. Master students are introduced to the field of Archaeometry that see the collaboration of experts in different areas of research such as conservators, curators…

By early spring 2020, the COVID-19 pandemic caused mandatory campus closures of academic institutions nationwide, prompting the rapid transition to online instruction. While lectures and exams were more straightforwardly administered online using video-chatting software, many hands-on laboratory-based courses were forced to develop creative…

The traditional methods of teaching organic chemistry laboratories do not seem to effectively promote content retention, communication skills, or valuable soft skills. The purpose of this convergent triangulation mixed-methods, scholarship of teaching and learning action research study was to differentiate the impact of expository laboratory…

Laboratory experimentation providing students with hands-on experiences can greatly enhance the teaching and learning of physics. However, traditional hands-on laboratories are very expensive, limiting the possibilities for practical activities. In addition, limited time for laboratory practices prevents teachers and students from conducting…

Laboratory courses can help students learn in a meaningful way. In the past, students encountered difficulties in chemistry laboratory courses due to limited access to equipment and space for practicing experimental operations. In recent years, virtual laboratories have allowed students to repeatedly practice in order to achieve their experimental…

Thermodynamic characterization of micelle formation from an ionic surfactant in aqueous solutions is a classic experiment in physical chemistry. The critical micelle concentration (CMC) and the degree of micelle ionization ([alpha)] can be directly obtained by conductimetry, then thermodynamic parameters ([delta]G[subscript m][superscript o],…

The free radical chlorination of an alkane experiment is often used in the undergraduate laboratory curriculum to introduce students to the free radical mechanism, substituent effects, intermediate stability, and the relative reactivity of radicals. In this experiment, students monochlorinate multiple alkanes and analyze the reaction mixture using…

Inductively coupled plasma optical emission spectroscopy (ICP-OES) is one of the most commonly used analytical techniques for the measurement of metals in environmental matrices. However, one of the drawbacks of ICP-OES is interference, viz., spectral and nonspectral (due to transport effects) interference. In this simple laboratory experiment,…

Keto-enol tautomerism is a special example of structural isomerism. In this experiment, 6-chlorofulvene is predominantly yielded during the chlorination reaction of 6'-hydroxyfulvene with POCl[subscript 3] in the presence of DMF. The high regioselectivity of this reaction is dominated by intramolecular hydrogen-bonding and steric hindrance,…

In this study a survey was developed to investigate students' engagement during general chemistry laboratory sessions. Aspects of engagement surveyed included cognitive, behavioral, and emotional engagement, and the survey items were focused on activities during the pre-laboratory introduction, laboratory procedures, and data collection.…

Although demonstrations play a central role in teaching and learning chemistry, the effects of concrete setup principles have rarely been subject to systematic empirical studies. According to the left-to-right principle, the educator should begin with the first step of a reaction in the upper left part of the setup and then place the following…

In this brief experiment, students create a superhydrophobic surface as an application of polar--nonpolar interactions and redox chemistry. Half of a zincgalvanized steel strip is coated in copper nanoparticles through electroless deposition. A layer of nonpolar octadecanethiol is added to half of that copper surface. Students classify the three…

Experimental electrochemistry offers unique opportunities for interactive instruction at all levels of education; however, widespread adoption in curricula is hindered by high costs associated with electrochemical instrumentation. Thus, the development of affordable instruments represents an essential step toward making electrochemistry accessible…

A laboratory activity is described for senior high school or first year undergraduate level students that illustrates key concepts linked to extractive metallurgy. This experiment demonstrates preferential binding of a methoxyphenolic oxime ligand to Cu[superscript 2+] in the presence of other transition metal ions in aqueous solution. The…

A simple one-dimensional [superscript 1]H NMR experiment that quantifies protein bound to gold nanoparticles has been developed for upper-division biochemistry and physical chemistry students. This laboratory experiment teaches the basics of NMR techniques, which is a highly effective tool in protein studies and supports students to understand the…