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An Operationally Simple Sonogashira Reaction for an Undergraduate Organic Chemistry Laboratory Class
Cranwell, Philippa B.; Peterson, Alexander M.; Littlefield, Benjamin T. R.; Russell, Andrew T. – Journal of Chemical Education, 2015
An operationally simple, reliable, and cheap Sonogashira reaction suitable for an undergraduate laboratory class that can be completed within a day-long (8 h) laboratory session has been developed. Cross-coupling is carried out between 2-methyl-3-butyn-2-ol and various aryl iodides using catalytic amounts of bis(triphenylphosphine)palladium(II)…
Descriptors: Undergraduate Study, College Science, Science Instruction, Organic Chemistry
Goldstein, Steven W.; Cross, Amely V. – Journal of Chemical Education, 2015
The reductive amination reaction between an amine and an aldehyde or ketone is an important method to add an additional alkyl group to an amine nitrogen. In this experiment, students react a selection of benzylamines with aldehydes to form the corresponding imines. These imines are reduced with a mixture of "p"-toluenesulfonic acid…
Descriptors: Organic Chemistry, Science Instruction, Science Experiments, Scientific Concepts
Usher, Karyn M.; Simmons, Carolyn R.; Keating, Daniel W.; Rossi, Henry F., III – Journal of Chemical Education, 2015
Chemical separations are an important part of an undergraduate chemistry curriculum. Sophomore students often get experience with liquid-liquid extraction in organic chemistry classes, but liquid-liquid extraction is not as often introduced as a quantitative sample preparation method in honors general chemistry or quantitative analysis classes.…
Descriptors: Science Instruction, College Science, Undergraduate Study, Chemistry
Holmes, N. G.; Lewandowski, H. J. – Physical Review Physics Education Research, 2020
Physics lab instruction is evolving in response to changing technology, a desire to better prepare students for diverse careers, and renewed focus from physics education researchers. To prepare researchers to evaluate progress in instructional labs in the future, this study set out to understand the current state of instructional physics labs in…
Descriptors: Physics, Laboratory Experiments, Teaching Methods, Science Instruction
Yearty, Kasey L.; Sharp, Joseph T.; Meehan, Emma K.; Wallace, Doyle R.; Jackson, Douglas M.; Morrison, Richard W. – Journal of Chemical Education, 2017
[Superscript 1]H NMR analysis is an important analytical technique presented in introductory organic chemistry courses. NMR instrument access is limited for undergraduate organic chemistry students due to the size of the instrument, price of NMR solvents, and the maintenance level required for instrument upkeep. The University of Georgia Chemistry…
Descriptors: Science Instruction, Organic Chemistry, Science Laboratories, Teaching Methods
Elias, Ryan J.; Hopfer, Helene; Hofstaedter, Amanda N.; Hayes, John E. – Journal of Food Science Education, 2017
The human nose is a very sensitive detector and is able to detect potent aroma compounds down to low ng/L levels. These levels are often below detection limits of analytical instrumentation. The following laboratory exercise is designed to compare instrumental and human methods for the detection of volatile odor active compounds. Reference…
Descriptors: Olfactory Perception, Human Body, Science Laboratories, Laboratory Procedures
Rosu, Cornelia; Cueto, Rafael; Veillion, Lucas; David, Connie; Laine, Roger A.; Russo, Paul S. – Journal of Chemical Education, 2017
Volatile compounds from polymeric materials such as weatherstripping were identified by solid-phase microextraction (SPME), a solvent-free analytical method, coupled to gas chromatography-mass spectrometry (GC-MS). These compounds, originating from additives and fillers used in weatherstripping processing, were mostly polycyclic aromatic…
Descriptors: Undergraduate Students, High School Students, College Science, Secondary School Science
Musik, Panjit – Turkish Online Journal of Educational Technology - TOJET, 2017
The development of computer-based experiment set has become necessary in teaching physics in schools so that students can learn from their real experiences. The purpose of this study is to create and to develop the computer-based experiment set on simple harmonic motion of mass on springs for teaching and learning physics. The average period of…
Descriptors: Science Experiments, Physics, Scientific Concepts, Motion
Johnson, Sadie M.; Javner, Cassidy; Hackel, Benjamin J. – Journal of Chemical Education, 2017
The goal of this study was to create an accessible, inexpensive, and engaging experiment to teach high school and undergraduate chemistry or biology students about intermolecular forces and how they contribute to the behavior of biomolecules. We developed an enzyme-linked immunosorbent assay (ELISA) to probe specific structure-function…
Descriptors: High School Students, Undergraduate Students, Chemistry, Molecular Biology
Affeldt, Fiona; Eilks, Ingo – School Science Review, 2018
Social media are a highly visible factor in the daily lives of our students. Why should teachers not take advantage of this and develop teaching and learning materials that use the designs found in such media to contextualise science learning? This article suggests some ideas for creating lab instructions using social media design as an innovative…
Descriptors: Internet, Social Media, Instructional Design, Science Instruction
Basso, A.; Chiorri, C.; Bracco, F.; Carnasciali, M. M.; Alloisio, M.; Grotti, M. – Chemistry Education Research and Practice, 2018
Improving the interest of high-school students towards chemistry (and science in general) is one of the goals of the Italian Ministry of Education. To this aim, we designed a context-based activity that actively involved students in six different laboratory experiences interconnected by a case study of the murder of Miss Scarlet, from the famous…
Descriptors: Foreign Countries, High School Students, Secondary School Science, Chemistry
Gülçiçek, Çaglar; Kizilcik, Hasan Sahin; Damli, Volkan – Physics Education, 2018
The purpose of this research is to determine the effects of different laboratory approaches on students' understanding of wave concepts. For this purpose, three experiments and experiment instructions have been designed for each of the three approaches (verification, hypothesis testing, and the 5E laboratory approach). Quantitative aspects of the…
Descriptors: Science Instruction, Scientific Concepts, Concept Formation, Science Laboratories
Tran, Khanh; Barrera, Ana Maria; Coble, Kim; Arreguin, Mireya; Harris, Marissa; Macha-Lopez, Alex; Perez, Michaela; Eroy-Reveles, Alegra – Physical Review Physics Education Research, 2022
At a large, diverse, hispanic-serving, master's-granting university, the Alma Project was created to support the rich connections of life experiences of science, technology, engineering, and mathematics (STEM) students that come from racially diverse backgrounds through reflective journaling. Utilizing frameworks in ethnic studies and social…
Descriptors: Cultural Capital, Algebra, Physics, Science Instruction
Rae, Guenevere; Cork, R. John; Karpinski, Aryn C.; Swartz, William J. – Anatomical Sciences Education, 2016
The purpose of this study was to design a one-hour brain dissection protocol for a medical neuroscience course and evaluate the short and long-term effects of its implementation on medical students. First-year medical students (n = 166) participated in a brain dissection activity that included dissection of the basal nuclei and associated deep…
Descriptors: Brain, Laboratory Experiments, Scores, Pretests Posttests
Gomes da Silva, Delmarcio; Menegatti de Melo, Fernando; Silveira, Alceu Totti, Jr.; Constancio da Cruz, Bruno; Prado, Caio Cesar Pestana; Pereira de Vasconcelos, Luana Cristina; Lucas, Vitor Amaral Sanches; Toma, Henrique Eisi – Journal of Chemical Education, 2016
A laboratory experiment has been developed to illustrate environmental and sustainability aspects, focusing on the wastewater treatment by means of superparamagnetic nanoparticles functionalized with humic acid. The experiment, conducted by a group of high school students, involves nanoparticle synthesis and minor characterization, followed by…
Descriptors: Science Instruction, Science Experiments, Laboratory Experiments, Science Laboratories

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