Size exclusion chromatography is an important technique in the separation of biological and polymeric samples by molecular weight. While a number of laboratory experiments have been published that use this technique for the purification of large molecules, this is the first report of an experiment that focuses on purifying an unknown small…

This paper begins with an early measurement of the speed of sound in water. A historical overview of the consequent development of SONAR and medical imaging is given. A method of measuring the speed suitable for demonstration to year 10 students is described in detail, and an explanation of its systematic error examined.

Poly(vinyl alcohol) (PVA) precipitates in many kinds of aqueous salt solutions. While sodium sulfate, a coagulant for PVA fiber, precipitates PVA to yield a white rigid gel, coagulation of PVA with aluminum sulfate, a coagulant for water treatment, yields a slime-like viscoelastic fluid. One type of homemade slime is prepared under basic…

A small-scale wastewater cleaning plant is described that includes the key physical pretreatment steps followed by the chemical treatment of mud by flocculation. Water, clay particles, and riverside deposits mimicked odorless wastewater. After a demonstration of the optimization step, the flocculation process was carried out with iron(III)…

Dark matter makes up most of the matter in the universe but very little of a standard introductory physics curriculum. Here we present our construction and use of a spandex sheet-style gravity simulator to qualitatively demonstrate two aspects of modern physics related to dark matter. First, we describe an activity in which students explore the…

Thin film interference manifests itself in a wide range of visually pleasing situations in everyday life (in the colored effects caused by a drop of oil on water, in soap bubbles, etc.) and is also involved in important technical applications (semi-reflecting mirrors, anti-reflection lenses, etc.). Yet, despite its familiarity, high school…

A contemporary approach to the synthesis and purification of several UV-active dipeptides has been developed for the second-year organic laboratory. This experiment exposes students to the important technique of solution-phase peptide synthesis and allows an instructor to highlight the parallel between what they are accomplishing in the laboratory…

When conducting experiments involving the measurement of physically related quantities, choosing an appropriate spacing for the experimental independent variable is a crucial procedure whose consequences may go beyond data graphical visualization. This is particularly true if the measured quantities are nonlinearly related and experimental errors…

An operationally simple, reliable, and cheap Sonogashira reaction suitable for an undergraduate laboratory class that can be completed within a day-long (8 h) laboratory session has been developed. Cross-coupling is carried out between 2-methyl-3-butyn-2-ol and various aryl iodides using catalytic amounts of bis(triphenylphosphine)palladium(II)…

The reductive amination reaction between an amine and an aldehyde or ketone is an important method to add an additional alkyl group to an amine nitrogen. In this experiment, students react a selection of benzylamines with aldehydes to form the corresponding imines. These imines are reduced with a mixture of "p"-toluenesulfonic acid…

Twenty-two hundred years ago, the Greek scientist Eratosthenes measured the circumference of the Earth. This paper describes an experiment to replicate Eratosthenes' experiment with observers located in Australia and New Zealand. The most accurate circumference produced in the experiment described in this paper is 38,874?km, measured at Rosebud,…

Chemical separations are an important part of an undergraduate chemistry curriculum. Sophomore students often get experience with liquid-liquid extraction in organic chemistry classes, but liquid-liquid extraction is not as often introduced as a quantitative sample preparation method in honors general chemistry or quantitative analysis classes.…

New and emerging digital technologies are making an impact on how we practice science, and this has implications on how we teach science. We introduce the concept of the Electronic Laboratory Notebook (ELN) as used in the research environment and describe how we have implemented this as a tool for providing undergraduate science students with an…

[Superscript 1]H NMR analysis is an important analytical technique presented in introductory organic chemistry courses. NMR instrument access is limited for undergraduate organic chemistry students due to the size of the instrument, price of NMR solvents, and the maintenance level required for instrument upkeep. The University of Georgia Chemistry…

The Canadian Remote Sciences Laboratories (CRSL) website (www.remotelab.ca) was successfully employed in a study of the differences in the performance and perceptions of students' about their learning in the laboratory (in-person) versus learning at a remote location (remote access). The experiment was completed both in-person and via remote…