The catalytic hydrogenation of alkenes and alkynes is an important part of the undergraduate chemistry curriculum and is a fundamental process in chemical industry. Inquiry-based laboratory activities are presented that investigate the hydrogenation of alkynes on a nanoparticle palladium surface to form alkenes, which go on to form alkanes. Alkyne…

This comprehensive experiment is specially designed for the third-year and above students who are majoring in chemistry, applied chemistry, and chemical engineering. Students conduct experiments in groups, which are required to synthesize the CeO[subscript 2]-NiTiO[subscript 3]/attapulgite (ATTP) composite catalyst by the sol-gel method; the…

Thermal conductivity is generally the tool of choice for quantification of fixed gases, particularly lighter-than-air gases. Unfortunately, gas chromatography-thermal conductivity detectors (GC-TCDs) are difficult to introduce in first- and second-year chemistry courses where the cost and number of instruments, as well as the space required, is…

The dynamics of a spring pendulum is an important topic in introductory experimental physics courses at universities and advanced science courses in secondary school education. Different types of pendulum setups with smartphones were proposed to investigate, e.g., the gravitational acceleration, to measure spring constants, or to illustrate and…

Herein we report the design of an upper-level hybrid laboratory course in the area of applied biopharmaceuticals, which has high scheduling flexibility, and utilizes both virtual and in-person educational elements to enhance students' learning experience. This newly developed course applies chemical engineering knowledge, practical and…

A laboratory experiment that involves the synthesis, characterization, and application exploration of a metal-organic framework (MOF) has been developed for first-year undergraduates in the Faculty of Engineering at National University of Singapore. The desired MOF material was prepared from commercially available reagents in a facile…

Biodiesel is an important biomass, largely employed in the transport sector and produced from vegetable oils. Additionally, waste cooking oils may be reused to produce biodiesel fuel, minimizing environmental pollution. A laboratory experiment that affords a widespread way to discuss degradation concepts and tools for used vegetable oil…

In this paper, the dynamic case of a system made up of two blocks connected by a string over a smooth pulley is revisited. One mass lies on a horizontal surface without friction, and the other mass has a vertical displacement. The motion equation is obtained and its solution is determined using the "Mathematica" package. Also an…

When injecting dye into a vortex, one finds that the dye remains captured around the vortex core over minutes, despite the fact that the vortex (and the dyed region) is strongly time-dependent. According to a recent theory, three-dimensional time-dependent vortices should be defined as rotating, material-holding regions of the fluid. Vortices…

Measuring the "e/m" ratio is a classic experiment in the physics curriculum. We show that smartphones can reliably measure the magnetic field strengths involved. Moreover, phone cameras and the image-processing software Tracker can make determining the charge-to-mass ratio of the electron more accurate.

The fact that a bungee jumper can reach an acceleration greater than the acceleration of gravity is, also from a physics point of view, intriguing. Taking only gravity into account, it can be explained by applying conservation of energy or by deriving carefully the equation of motion in a Newtonian approach. In this article we show how it can be…

Carbohydrates are an essential group of molecules to the organic chemistry classroom providing molecular relevance to a common ingredient in chemical biology. While the meticulous elucidation of the carbohydrate structures by Fischer and others is an engaging topic in the lecture, there are few laboratory experiments that can emulate carbohydrate…

A continuous flow photopinacol coupling of benzophenone has been developed and implemented in the undergraduate laboratory. This photoreduction was accomplished using 2-propanol as an H atom donor and cosolvent in the reaction. The simple and inexpensive UV light source and flow reactor design (less than $350/photochemical flow system) provide an…

Williamson ether experiments are commonly performed by students in undergraduate organic chemistry instructional laboratory courses. In this multioutcome experiment, students were provided 4-bromophenol and one of three alkyl halides: 1-bromopentane, 1-bromobutane, or 1-bromo-3-methylbutane. The alkyl halides served as the unknown component of the…

Interfacial solar vapor generation has recently drawn much attention because of its high solar-to-vapor generation efficiency. Here we introduce the basic experimental procedures and analysis for undergraduates to perform such an experiment to catch up with the cutting-edge research wave. Interfacial solar vapor generation employs an interfacial…