Education reform calls for portraying science as a process of inquiry and argumentation grounded in the epistemic traditions of a domain. While experimentation is a core scientific investigation strategy, diverse approaches are represented across different domains of science. Ecosystem scientists use experiments as a core part of their…

The discovery of ferrocene, Fe(C[subscript 5]H[subscript 5])[subscript 2], in the 1950s sparked the development of organometallic chemistry including metallocene compounds. Shortly after the isolation of ferrocene, the analogous ruthenium and osmium compounds were discovered. The preparation of ferrocene is common in undergraduate inorganic…

Metal-organic frameworks (MOFs) are a class of porous materials that are often crystalline with high surface area and structural tunability. In this laboratory experiment designed for inorganic chemistry students at the undergraduate level, students complete a two-step experiment where they will first (i) synthesize two isostructural…

Previous educational articles on microfluidic technology mainly focused on continuous microfluidics, so we set up an undergraduate laboratory experiment to introduce droplet microfluidics to students. Students can understand the concept of microfluidic channels and the principles of droplet microfluidics, prepare polydimethylsiloxane (PDMS)…

The addition of a small excess of triethyl orthoformate to an alcoholic mixture of NiCl[subscript 2]·6H[subscript 2]O and triphenylphosphine (PPh[subscript 3]) results in an increase in the typical isolated yield of [NiCl[subscript 2](PPh[subscript 3])[subscript 2]] from below 50% to over 85%. The impact of water when present in the reaction…

The formation of chemical patterns is in general difficult to control due to the random diffusive motions of the reacting chemical species in solution. In this paper, we present a new method using audible sound to control the formation of chemical patterns obtained in blue bottle experiments. The waves generated on the surface of the solution by…

Electrochemistry represents a powerful sustainable method for chemical synthesis; however, its widespread application is limited due to the lack of exposure and appropriate basic training of synthetic chemists and engineers in electrochemistry and electrochemical engineering. The introduction of diverse laboratory practices to the current…

We investigated a very long chain falling from the pile on the edge of a table to the floor both experimentally and theoretically. In this very simple and novel configuration we showed that the velocity of the chain quickly converges to its asymptotic value, and that the steady-state velocity is proportional to the square root of the height of the…

The measurement of the charge-to-mass ratio, e/m, of the electron is a fundamental part of any study of electricity and magnetism. It is possible to use an apparatus designed to measure e/m for other things, including investigations of electron flow through a near vacuum, measuring a work function, and even exploring some quantum mechanics…

Our first experience of dimension typically comes in the intuitive Euclidean sense: a line is one dimensional, a plane is two dimensional, and a volume is three dimensional. However, following the work of Mandelbrot, systems with a fractional dimension, "fractals," now play an important role in science. The novelty of encountering…

In this paper, a simple method is described for visually demonstrating that the wavelength of light reduces when entering a medium of higher refractive index. When a violet laser (405 nm) is reflected off the surface of a Blu-ray disc (track spacing 320 nm) diffraction cannot occur since the wavelength is greater than the track spacing. However,…

Students determine the iron mass in dietary supplements using four colorimetric assays. These colorimetric assays were selective for Fe[superscript 3+]. It was complexed by thiocyanide, salicylate, gallic acid, and Fe(CN)[subscript 6][superscript 4-], forming blood-red, red, violet, and blue complexes, respectively. The [lambda][subscript max] of…

Applying the idea of green chemistry, we extended an esterification teaching experiment with isoamyl alcohol and acetic acid and reused isoamyl acetate in the transesterification reaction with KOH as the catalyst. As a result, isoamyl alcohol was produced and could be reused for the teaching experiment. The simplified experimental method achieved…

Benzoin, an [alpha]-hydroxy ketone, is stereoselectively reduced by sodium borohydride to yield hydrobenzoin, the stereochemistry of which is determined by acetalization and analysis of the derivative by NMR spectroscopy. This classical experiment has been enhanced by modern spectroscopic and computational analysis to enable students to…

Experiments are considered to be essential components of science learning. This research aimed to investigate trends in the use of science experiments in online learning. A systematic literature review was carried out, with data sourced from the Scopus and Google Scholar databases. The reviewed documents were journal articles published between…