Use of combined liquid chromatography and finite-current electrochemistry (LCEC) procedures are discussed. Also discusses the relationship between electroactivity and molecular structure, selectivity in LCEC, and LCEC applications. Because of its selectivity and low detection limits, the procedures are most often applied in biomedical and…

Describes a course designed to provide secondary school science teachers with the background necessary to implement an effective safety program for their science labs. Lectures, demonstrations, group discussions, slides, films, videotapes, and guest speakers were utilized in the two-credit hour, summer course. Evaluations indicated course…

Reviews trends in liquid chromatography including apparatus, factors affecting efficient separation of a mixture (peak sharpness and speed), simplified problem-solving, adsorption, bonded phase chromatography, ion selectivity, and size exclusion. The current trend is to control chemical selectivity by the liquid phase. (Author/JN)

Use of gradient elution techniques in high performance liquid chromatography (HPLC) is often essential for direct separation of complex mixtures. Since most commercial controllers have features that are of marginal value for instructional purposes, a low-cost controller capable of illustrating essential features of gradient elution was developed.…

Describes an inexpensive means for determining proximate analysis of coal, and by use of this data, its energy content. Pyrite content is also obtained by utilizing magnetic properties of iron. The simple device used makes the experiment suitable for the undergraduate laboratory. (Author/JN)

Briefly reviews some optical and other physical properties of minerals that can be determined in reflected/incident light. Topics include optical properties of minerals, reflectance, internal reflections, color, bireflectance and reflection pleochroism, anisotropism, zonation, and reflected light microscopy as a teaching tool in undergraduate…

Describes an experiment presented to students as a problem in determining the stoichiometry of "copper iodide" to decide whether it is cuprous iodide or cupric iodide. The experiment illustrates stoichiometry principles, providing experiences with laboratory techniques and numerical computation. Detailed outline (written for student use) is…

"Anodizing Aluminum" (previously reported in this journal) describes a vivid/relevant laboratory experience for general chemistry students explaining the anodizing of aluminum in sulfuric acid and constrasting it to electroplating. Additions to this procedure and the experiment in which they are used are discussed. Reactions involved are…

Describes a laboratory experiment which introduces basic principles and experimental techniques of mass spectrometry for fourth year undergraduate (B.Sc.) students. Laboratory procedures, background information, and discussion of results are provided for the experiment in which the natural isotopic abundance of chlorine is determined. (Author/JN)

Describes an experiment using a high-speed preparative centrifuge and calculator to demonstrate effects of the frictional coefficient of a macromolecule on its rate of transport in a force field and to estimate molecular weight of the macromolecule using an empirical relationship. Background information, procedures, and discussion of results are…

Much of the stress on teachers and students during clothing construction laboratories can be eliminated by (1) appropriate planning, including selection of objectives, choice of projects, and well-defined grades; (2) classroom management, including organization of time, space, equipment, and students; and (3) alternation of demonstrations and…

Reviews Hanson's findings that laboratory research tends to demonstrate a positive correlation between attitudes and behavior while field research does not. This article, by adding date of publication, shows that the trend over time, presumably because of improved methodology, is toward more positive correlations in both settings. (Author/JAC)

Discusses ways to combine technological innovations in the areas of visual aids and computers with existing language lab equipment in order to motivate students in the area of second language learning. (EKN)

Describes a modified version of an experiment found in the laboratory manual "Chemistry" by Masterton, Slowinski, and Wolford (Holt, Rinehart and Winston, 1980). Accurate results (normally less than four percent error) in less time were achieved when magnesium turnings were used instead of magnesium ribbon called for in the original experiment.…

Describes modifications of a Nuffield experiment demonstrating oxygen transport by blood since the current experiment more often than not produces unsatisfactory results. Includes experimental modification, instructional strategy, assembly of equipment, and a brief discussion. (JN)