The electrical properties of polyaniline changes by orders of magnitude upon exposure to analytes such as acids or bases, making it a useful material for detection of these analytes in the gas phase. The objectives of this lab are to synthesize different diameter polyaniline nanofibers and compare them as sensor materials. In this experiment…

Provides a listing of all state guidelines and regulations pertaining to use of hypodermic syringes, eye safety, and animal care in biology and general science laboratories. (SL)

Studies from our laboratories over recent years have uncovered the existence, and established the properties of a variety of mitochondrial transporters. The properties of these transporters throw light on a variety of biochemical phenomena that were previously poorly understood. In particular the role of mitochondrial transport in energy…

In this work, we present a simple analysis of binary diffraction gratings with different slit widths relative to the grating period. The analysis is based on a simple phasor technique directly derived from the Huygens principle. By introducing a slit phasor and a grating phasor, the intensity of the diffracted orders and the grating's resolving…

The conceptual understanding of Archimedes' principle can be verified in experimental procedures which determine mass and density using a floating object. This is demonstrated by simple experiments using graduated beakers. (Contains 5 figures.)

Various water-alcohol and alcohol-alcohol based experiments are used to demonstrate how the quartz-crystal microbalance (QCM) technique is used for measuring the viscosity of a system. The technique is very advantageous, as it is inexpensive and provides digital output.

A lab practical exam for second-year organic chemistry is presented that tests multiple lab skills and theory that the students have acquired directly from laboratory experiences. This exam motivates students to learn lab skills and is an effective end-of-term test for many of those skills. (Contains 2 figures.)

We present a new laboratory experiment on the photochemistry of organometallic [eta][superscript 5],[eta][superscript 6]-mixed-sandwich compounds, which is suitable for both the physical chemistry and inorganic chemistry laboratory. Specifically, students use 1,10-phenanthroline to trap the intermediate formed when…

The nitration of six benzene derivatives having a range of substituents that differ in electronic effects were followed by GC-MS analyses of the crude reaction mixtures and adapted for the second-year organic laboratory. Students pool their results and identify the products by analyzing the mass spectral data of the isomers and by comparing them…

The experiment demonstrating the feasibility of using water as a solvent for organic reactions which highlights the cost and environmental benefits of its use is presented. The experiment encourages students to think in terms of the reaction mechanism of the oxidation of aldehydes knowing that potassium persulfate is the active oxidant in Oxone…

Preparation of phenylmagnesium bromide described by Eckert, addition of three equivalents of Grignard reagent to diethyl carbonate to form triphenylmethanol and a series of GC-MS procedures that form intermediates. The analysis is consistent with a gas chromatogram and mass spectrum for each of the expected intermediates and final product of the…

Technical education is, by definition, a field that requires hands-on practice and experience by the student. When it comes to distant learning, technical education suffers from lack of such practical study, given the fact that e-learning is based on theoretical material being provided remotely to the student. This article presents the idea of…

A simple laboratory exercise is illustrated that exposes students to wide range of separation techniques in one laboratory program and provides a nice complement to a project-oriented program. Students have learned the basic principles of syringe filtration, centricon, dialysis, gel filtration and solid-phase extraction methodologies and have got…

The cAcL[subscript 2] approach (concept Advancement through chemistry Lab-Lecture) incorporates three major educational methodologies into one: a student-centered approach, the full integration of lecture and laboratory formats, and hands-on activity based-instruction. This format has been tested for cognitive and attitudinal gains in students and…